---
title: Double tilt LN2 Vacuum Transfer Holder | Mel-Build
description: This is the only TEM holder in the world created for the study of lithium-ion batteries. Vacuum transfer is possible and cooling is possible to reduce electron beam damage. In addition, it is equipped with a double tilt mechanism to match the crystal orientation, making it the only TEM holder in the world that allows atomic resolution observation. The temperature stability is ± 0.005degreeC and it has a tremendous temperature control ability.
image: https://melbuild.com/hubfs/melbuild.com/images/common/ogp.png
---

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          - [Double tilt 4 Electrodes Transfer Holder](https://melbuild.com/vacuum-transfer-3rd)
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# Double tilt LN2 Vacuum Transfer Holder

- ![Double tilt LN2 Vacuum Transfer Holder](https://melbuild.com/hubfs/melbuild.com/images/vacuum-transfer-1st/img_vacuum-transfer-1st01.png)

LN2 Cooling -160°C + Double tilt±20° + Vacuum Transfer TEM holder  
Get the High Resolution image and EDS Analysis at-160°C  
Temp. Control ±0.005°C

## - High Resolution at -160°C data movie and data Collection -

![img_vacuum-transfer-1st02-1](https://melbuild.com/hubfs/melbuild.com/images/vacuum-transfer-1st/img_vacuum-transfer-1st02-1.gif)

### Sample：Au nanoparticles ARM 200F in Kyushu University

Factory check resolution image

![ (La,Li)TiO3 University of Tokyo](https://melbuild.com/hubfs/melbuild.com/images/vacuum-transfer-1st/img_vacuum-transfer-1st03.gif)

### Sample：(La,Li)TiO3 University of Tokyo

Dr. Ishikawa Dr. Nakayama  
Prof. Shibata Prof. Ikuhara

![SrTiO3 University of Tokyo](https://melbuild.com/hubfs/melbuild.com/images/vacuum-transfer-1st/img_vacuum-transfer-1st04.gif)

### Sample：SrTiO3 University of Tokyo

Dr. Ishikawa Dr. Nakayama, Dr. Kumamoto  
Prof. Shibata Prof. Ikuhara

- ![冷却 LLZ-1](https://melbuild.com/hubfs/%E5%86%B7%E5%8D%B4%20LLZ-1.png)

Atomic resolution STEM image observation of LLZ(Li7La3Zr2O12),which is degraded by exposure to air(moisture) and weak to electron beam with lithium ion material, was successful.  
From this result, it was proved that the non-exposure(Transfer) was successful, and the crystal orientation was adjusted by Y tilt,and the electron beam damage was reduced by cooling of -160°C.

 

## - Reasons for high-resolution image at -160°C -

We realized it with the following our special system.

1. Mechanical drift cancellation mechanism from our patented technology
2. High-precision temperature controller. Range is ± 0.005°C.
3. Original Gonio cover for cryo tem holder

By making these into one system, it is possible to obtain much easier get the high resolution  
image than current cooling holders.

- ![Cryo vacuum transfer tem holder](https://melbuild.com/hubfs/melbuild.com/images/vacuum-transfer-1st/img_vacuum-transfer-1st07.png)

As a result, the stability during cooling has improved, so we have successfully acquired EDS column map data.

- ![Cryo vacuum transfer tem holder](https://melbuild.com/hubfs/melbuild.com/images/vacuum-transfer-1st/img_vacuum-transfer-1st08.png)

EDS analytical performance test using LN2 cooling holder：Column mapping of SrTiO3

Annotation: Observations using this holder are dependent on specific cooling conditions and are influenced by the TEM environment. Therefore, it cannot be guaranteed that identical data will be obtained in all environments.

## TEM holder Specification

 

| Component | Vacuum Transfer / Double tilt / Cooling |
| --- | --- |
| Ultimate temp. ※Guarantee temp. | -165±5℃ |
| Arrival time | 60 min. |
| Tilt Angle | JEOL:X:± 25 degree  , Y:± 20 degree  @ HR PP               ± 10 degree  , Y:± 7 degree @ HR PP  FEI:X:± 30 degree, Y:± 20 degree  @ ST PP |
| Resolution | 0.24nm 　Au Nano Particle TEM FFT 002 observation 0.14nm (Factory check specification) |
| Drift Rate | 5 nm/min.　※TEM room noise less than 50db |

## Safety Operation Stand of tem holder introduce

- ![Cryo vacuum transfer tem holder](https://melbuild.com/hubfs/melbuild.com/images/vacuum-transfer-1st/img_vacuum-transfer-1st10.png)

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